Hydrothermal synthesisreactortseem hu ua microreactor lossis lub nkoj siab. Piv nrog rau lwm cov reactors, nws muaj tus nqi qis thiab cov qauv yooj yim. Nws siv cov hlau tsis muaj hlau ua cov khoom tiv thaiv siab thiab yog kab nrog polytetrafluoroethylene. Nws yog tsim nyog rau cov tshuaj tiv thaiv ntawm ntau yam muaj zog acids, muaj zog alkalis thiab lwm yam xov xwm. Nws muaj kev huv huv siab thiab tsis muaj kuab paug corrosion. Nws tuaj yeem siv rau kev ntsuas cov tshuaj tiv thaiv ntawm tib cov khoom nruab nrab nyob rau hauv cov xwm txheej sib txawv, thiab nws kuj tuaj yeem siv rau kev ntsuas tshuaj tiv thaiv ntawm cov khoom sib txawv ntawm cov khoom sib txawv raws li tib yam.
Qhov filling degree yog dab tsi? Lub filling degree hais txog qhov feem pua ntawm cov kua ntim rau qhov ntim ntawm hydrothermal decomposition reactor. Piv txwv li, rau 100ml hydrothermal synthesis reactor, 80ml ntawm cov kua yog poured rau hauv lub reactor hauv ob sab phlu, uas yog, lub filling degree yog 80%.
Qhov tseeb filling degree ntawm hydrothermal synthesis reactor yog 60% ~ 80%. Yog hais tias lub solubility ntawm ligand yog me me, lub filling degree yuav loj me ntsis, thiab lub siab yuav nce raws li, tab sis nws yuav tsum tsis txhob muab sau ntau dhau lawm, txwv tsis pub thaum lub siab nce mus rau theem uas lub reactor hloov mus rau ib tug series. ntawm cov xwm txheej xws li kev puas tsuaj ntawm lub reactor yuav tshwm sim. Kev nyab xeeb yog qhov tseem ceeb hauv kev ua haujlwm. Ntawm chav kawm, yog tias koj xav txhob txwm kho lub siab nyob rau hauv lub reactor, ntxiv rau nce lub filling degree, koj tuaj yeem txiav txim siab ntxiv qee cov kuab tshuaj inorganic rau cov dej hnyav, lossis ncaj qha cuam tshuam rau qee feem ntawm cov kuab tshuaj sib xyaw, tab sis ua tib zoo mloog. kev khiav hauj lwm kub thiab tsis ua hauj lwm sab nraum lub reactor kub ntau yam.
Feem ntau, kev sau qib ntawm li 70% yog qhov tsim nyog dua. Qhov thib ob, xav txog seb qhov solubility ntawm lub ligand loj los yog me me, thiab tom qab ntawd kho cov qib filling thiab siab raws li qhov tseeb qhov ntsuas kub.
Yuav ua li cas los txiav txim siab qhov filling degree ntawm lub reactor feem ntau txiav txim siab los ntawm cov kuab tshuaj thiab cov tshuaj tiv thaiv kub ntawm qhov kev sim tshuaj tiv thaiv.
1. Qhov sib xyaw coefficient ntawm cov khoom siv tshuaj tiv thaiv hauv lub reactor feem ntau yog 0.6-0.85;
2. Yog hais tias cov khoom nyob rau hauv ib tug foamy los yog boiling xeev thaum lub sij hawm cov tshuaj tiv thaiv, nws yog feem ntau yog 0.6-0.7;
3. Yog hais tias cov khoom yog volatile heev thaum lub sij hawm cov tshuaj tiv thaiv, nws yog feem ntau 0.8-0.85;
Kev sau qib ntawm hydrothermal synthesis reactor yuav tsum tau txiav txim siab raws li kev sib cuag ntawm lub reactor thiab lwm yam kev ua haujlwm. Nws yuav tsum tsis tsuas yog ua tau raws li qhov ua tiav ntawm cov tshuaj tiv thaiv, tab sis kuj xyuas kom meej tias cov khoom sib xyaw kom txaus thiab tsis dhau.
